What error is introduced if the volume of the sample is determined first
If the volume of a sample is determined first, you would have a 'random error'. The error will still be present, but its magnitude will be such a small fraction of the value that it will not be detected, and cause problems for later calculations.
Random error
If the volume of the sample is determined first then there can be a random error occur. Because volume can change during the process so it should be measured first.